Identification of a new class of thermolabile psychoactive compounds, 4-substituted 2-(4-X-2, 5-dimethoxyphenyl)-N-[(2-hydroxyphenyl)methyl]ethanamine

Forensic Chemistry

Available online 19 July 2020, 100266

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Identification of a new class of thermolabile psychoactive compounds, 4-substituted 2-(4-X-2, 5-dimethoxyphenyl)-N-[(2-hydroxyphenyl)methyl]ethanamine (25X-NBOH, X= Cl, Br, or I) by gas chromatography-mass spectrometry using chemical derivatization by heptafluorobutyric anhydride (HFBA)

Benny J.LumaThomas A.BrettellbJoseph J.BrophycD.Brynn Hibbertc


https://doi.org/10.1016/j.forc.2020.100266Get rights and content

Highlights

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Paper describes method which can expand the analytical ability of traditional gas chromatography-mass spectrometry (GC-MS)

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Addresses concerns with specific compounds that are thermal labile such NBOHs and amphetamines.

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HFBA chemical derivatization is extremely sensitive, robust and reproducible and is a great consideration as a confirmatory method.

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This HFBA method can be applied to compounds such as phenethylamines, substituted cathinones or other forensic significant compounds.

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